Showing 3 results for Hussain
Farah Hanani Zulkifli, Hamid Hazrulrizawati , Fathima Shahitha Jahir Hussain, Nur Fatini Ilyana Mohamat Johari,
Volume 21, Issue 2 (June 2024)
Abstract
Researchers are increasingly focusing on green synthesis methods for silver nanoparticles due to their cost-effectiveness and reduced environmental impact. In this study, we utilized an edible bird's nest (EBN), a valuable economic resource, as the primary material for synthesizing silver nanoparticles using only water as the solvent. Metabolite profiling of the EBN extract was conducted using LC-QTOF-MS in positive mode (ESI+), revealing the presence of lipids, glycosides, peptides, polysaccharides, and disaccharides. Upon the addition of silver nitrate to the aqueous EBN extract, noticeable color changes from transparent to brown indicated the successful formation of AgNPs. Subsequent characterization of these silver nanoparticles involved UV-Visible spectroscopy, which revealed an absorption peak at 421 nm. Further characterization was carried out using FESEM, ATR-FTIR spectroscopy, and EDX analysis. The involvement of phenolic agents, proteins, and amino acids in reducing the silver particles was confirmed. The synthesized nanoparticles exhibited a spherical shape, and a particle size ranging from 10 to 20 nm. The presence of elemental silver was confirmed by a strong, intense peak around 3 keV in the EDX spectrum. To assess their potential, the antibacterial properties of the silver nanoparticles against Escherichia coli and Staphylococcus aureus were evaluated using the agar diffusion method.
Faraz Hussain, Muhammad Umar Manzoor, Muhammad Kamran, Tahir Ahmad, Fahad Riaz, Sehrish Mukhtar, Hafiz Muhammad Rehan Tariq, Muhammad Ishtiaq,
Volume 21, Issue 3 (September 2024)
Abstract
Magnesium alloys are increasingly valued for biomedical applications due to their biocompatibility. This study investigates Mg-AZ31B alloy samples treated with quartz and alumina grits (<200 μm) at varied pressures, followed by anodization in an eco-friendly alkaline electrolyte. The results show that increased blasting pressure produces a rougher surface. Anodization time significantly affects the thickness of the anodic film, leading to a transition in surface morphology from fine to coarse structures with complete film coverage. Characterization by XRD reveals that the anodic film mainly comprises magnesium oxide and hydroxide phases. Open Circuit Potential (OCP) measurements demonstrate enhanced corrosion resistance post-anodization, particularly notable at 40 minutes on alumina-blasted samples. ANOVA confirms that both blasting pressure and anodization time significantly influence coating thickness and OCP, indicating the formation of a dense anodized layer.
Zainab T Hussain, Wasna’a M Abdulridha, Murooj A Abood, Farqad Saeed,
Volume 23, Issue 1 (MARCH 2026)
Abstract
In this study, RF magnetron sputtering was employed to create titanium dioxide (TiO2) thin films doped with zirconium oxide (ZrO2) (TZO) onto quartz and silicon substrates at 100oC for the purpose of evaluating the effect of ZrO2 doping on the microstructural, electrical, optical and gas sensing properties of the TiO2 films. Different doping concentrations (0.0, 2.0 and 4.0 wt.%) were used to compare performances of the films with a thickness ranging between 147 nm to 178 nm. Structural and surface morphology characterizations of the prepared films were carried out by X-ray diffraction (XRD) and atomic force microscopy (AFM) techniques. The surface morphology of the prepared TZO films showed a gradual reduction in the grain size while the doping concentration increased. The optical characteristics of the films also exhibited an increasing trend in the optical band gap with the rising ZrO2 concentration. TiO2 films showed an n-type conductivity as confirmed by Hall's measurement. The results of the gas sensing experiments revealed that the sensitivity of the TZO films for the detection of ethanol vapor increased with an increase in the concentration of ZrO2 dopant. Therefore, TZO film with 4.0 wt.% of ZrO2 could be used as an effective sensor for detecting ethanol vapor.
