Showing 3 results for Sem.
A. Nemati, K. Pourazarang,
Volume 5, Issue 3 (9-2008)
Abstract
Abstract: The PZT-based ceramics with a composition of Pb1.1-xLax (Zr0.53Ti0.47)O3, were prepared
by conventional mixed oxide followed by mechanical alloying and sol-gel methods in which x was
chosen in the range of 0.02–0.06. The samples were calcined in the range of 450 °C - 750 °C for
4h. The physical and electrical properties of the samples were determined as a function of the
calcination temperature. The obtained data from two methods were compared with conventional
mixed oxide method. Microstructural and compositional analyses of the samples were carried out
using XRD and SEM. Dielectric properties of the samples were measured with an impedance
analyzer. The ferroelectric properties of the PZT and PLZT samples were measured using the
frequencies applying equipment and d33 tester. The results indicated a complete tetragonal phase
prepared from both methods. It was shown that the addition of La and reduction in calcination
temperature improved both the dielectric and piezoelectric properties. The dielectric constant
tended to increase with doping content, giving the maximum value of about 2000 at 3 mol% La3+.
In addition, the mechanical coupling factor (Qm) of the doped samples showed a significant
decrease. Finally, the value of planar coupling factor (kp) reached the maximum value of 0.47 at 1
mol% La3+.
A. A. Hosseini, A. Sadigzadeh, S. Mohammadi,
Volume 8, Issue 3 (9-2011)
Abstract
Abstract: In this study, carbon nanotubes (CNTs) were grown directly in the pores of micro porous pyrex membranes
and consequently ceramic membranes with very fine pores and high porosity were achieved. Our experiment was done
in two stages. Initially cobalt powder with different percent was homogeneously mixed with pyrex powder. In order to
produce row membranes, each of these mixtures were compacted in the form of tablet by use of a uniaxial cold press
and in a stainless steel mould, and then the tablets were sintered at different temperature in an electric furnace. In
second stage chemical vapor deposition (CVD) method was used to grow CNTs within the pores of the membranes.
Argon and ammonia were used as carrier and reactive gas respectively and acetylene was used as the carbon
feedstock. Morphology of the membranes before and after CVD process was studied by scanning electron microscopy
(SEM). After CVD process CNTs were grown in the pores of membranes and the pores size was decreased but total
porosity of the membrane was not changed considerably. In this way membranes with high porosity and fine pores were
fabricated.
S. Akbarzadeh, S.r. Allahkaram, S. Mahdavi,
Volume 15, Issue 2 (6-2018)
Abstract
Tin-Zinc alloy coatings have many applications because of their unique properties such as corrosion resistance, solderability and flexibility. In this study, the effect of current density, temperature and pH on chemical composition, cathodic current efficiency, morphology and structures of the coatings was investigated. The results illustrated that, at low current densities (<0.5 mA/cm2), the coatings were relatively pure tin, but Zn content increased with enhancing the current density. At higher currents a relatively pure Zn film was obtained. Temperature and pH also affected chemical composition of the alloy films. Zn content of the coatings was decreased by increasing the temperature, while its variation with pH had ascending-descending trend. Morphological investigation of the coatings revealed that increasing Zn content of deposits led to porous, rough and fine grained films.
