Resonance Phenomenon and Structural Properties of Fe Substituted Pzt Ceramics Prepared by Sol-Gel Method

Malika, AHABBOUD; Gouitaa, Najwa; fatimazahra, Ahjyaje; Taj-dine, Lamcharfi; Farid, Abdi

doi:10.22068/ijmse.2938

Volume 20, Issue 1 (March 2023) IJMSE 2023, 20(1): 1-14 | Back to browse issues page

‎ 10.22068/ijmse.2938

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Malika A, Gouitaa N, fatimazahra A, Taj-dine L, Farid A. Resonance Phenomenon and Structural Properties of Fe Substituted Pzt Ceramics Prepared by Sol-Gel Method. IJMSE 2023; 20 (1) :1-14
URL: http://ijmse.iust.ac.ir/article-1-2938-en.html

Resonance Phenomenon and Structural Properties of Fe Substituted Pzt Ceramics Prepared by Sol-Gel Method

AHABBOUD Malika

, Najwa Gouitaa

, Ahjyaje Fatimazahra

, Lamcharfi Taj-dine

, Abdi Farid

Abstract: (4817 Views)

In this paper, Pb_1-xFe_x(Zr_0.52Ti_0.48)O₃(PFZT) nanopowders, with x from 0.00 up to 0.20, were synthesized by using the sol-gel method. The PFZT samples were characterized by X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscopy (SEM), and impedance spectroscopy. According to the experimental results, PFZT combines rhombohedral and tetragonal symmetries for all the samples without a change in phase structure. The SEM investigation indicated that the grains are homogeneous with regular form and the average grain size of PFZT ceramics changed with Fe concentration. The dielectric characterizations show that the dielectric permittivity increases with increasing temperature, and the Fe amount shifts down the temperature of transition. Moreover, a dielectric resonance phenomenon is observed for all the PFZT ceramics.

Keywords: Pb1-xFex(Zr0.52Ti0.48)O3, X-ray diffraction, Raman spectroscopy, dielectric permittivity